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Binary Lead Fluoride Pb3F8
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DOI：10.1002/chem.201903954.png)
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摘要
En 中文
The binary lead fluoride Pb3F8 was synthesized by the reaction of anhydrous HF with Pb3O4 or by the reaction of BrF3 with PbF2. The compound was characterized by single-crystal and powder X-ray diffraction, IR, Raman, and solid-state MAS F-19 NMR spectroscopy, as well as thermogravimetric analysis, XP and near-edge X-ray absorption fine structure (NEXAFS) spectroscopy. Solid-state quantum-chemical calculations are provided for the vibrational analyses and band assignments. The electronic band structure offers an inside view of the mixed valence compound.
Keyword:
IR and Raman spectroscopy
lead fluoride
NEXAFS
NMR spectroscopy
quantum chemical calculations
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IF:
3.7
论文数:
3.9W
被引数:
10.5W
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