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High efficient synthesis of HMX from DPT using deep eutectic catalyst

delete2025-09-01
delete0
PRE
AI
H
Hu, Jianjian
D
Dapeng Jiang
Y
Yujie Huang
X
Xixue Liu
S
Shenyuan Gao
吴
吴可君 (Ke‐Jun Wu)
C
Chaohong He
L
Liyan Dai *
DOI：10.1016/j.tet.2025.134936delete
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摘要

摘要

En 中文
一种由深共熔催化剂（DEC）催化的硝化反应已用于从3,7-二硝基-1,3,5,7-四氮杂双环[3,3,1]壬烷（DPT）合成1,3,5,7-四硝基-1,3,5,7-四唑烷（HMX），该反应使用较少量的发烟硝酸并实现了最大产率85.8%。此外，DEC的引入显著提高了含氮底物（如双吗啉基甲烷和双哌啶基甲烷）的硝化效率，显著增加了其对应亚硝基产物的产率。该方法为基于离子液体的工艺提供了一种更绿色、更经济的替代方案。
Keyword:
NITROLYSIS
HEXAMETHYLENETETRAMINE
EXTRACTION
LIGNIN

期刊

T
Tetrahedron
IF:
2.2
论文数:
243
被引数:
3.3W

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暂无机构信息
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