.png){kind=icon}
返回
SASSY NMR: Simultaneous Solid and Solution Spectroscopy
.png){kind=icon}
PRE
AI
DOI：10.1002/anie.202216105.png)
.png){kind=icon}
原文求助.png){kind=icon}
分享.png){kind=icon}
收藏
摘要
En 中文
Synergism between different phases gives rise to chemical, biological or environmental reactivity, thus it is increasingly important to study samples intact. Here, SASSY (SimultAneous Solid and Solution spectroscopY) is introduced to simultaneously observe (and differentiate) all phases in multiphase samples using standard, solid-state NMR equipment. When monitoring processes, the traditional approach of studying solids and liquids sequentially, can lead to information in the non-observed phase being missed. SASSY solves this by observing the full range of materials, from crystalline solids, through gels, to pure liquids, at full sensitivity in every scan. Results are identical to running separate C-13 CP-MAS solid-state and C-13 solution-state experiments back-to-back but requires only a fraction of the spectrometer time. After its introduction, SASSY is applied to process monitoring and finally to detect all phases in a living freshwater shrimp. SASSY is simple to implement and thus should find application across all areas of research.
Keyword:
In Vivo
Liquid-State NMR
Multiphase Process Monitoring
NMR Spectroscopy
Solid-State NMR
期刊
IF:
16.9
论文数:
5.7W
被引数:
53.0W
机构
引用论文
Polyoxometalates on Functional Substrates: Concepts, Synergies, and Future Perspectives.png)
ADVANCED SCIENCE
OAAI
ADVANCED SCIENCEIF14.1
OAAI分享收藏From Spill to Sequestration: The Molecular Journey of Contamination via Comprehensive Multiphase NMROAAI
OAAI分享收藏分享收藏分享收藏
查看更多内容