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Selective N2 evolution from urea electrooxidation using NiCo2O4/activated carbon anode assisted by bipolar membrane under neutral conditions
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DOI：10.1016/j.seppur.2026.139634.png)
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Abstract
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• A BPM-assisted system enables efficient urea oxidation in neutral electrolyte. • Local alkaline microenvironment is created without bulk pH elevation. • 10%NiCo2O4/AC achieves 91.3% urea removal at 40 mA cm−2. • Selective nitrogen conversion to N2 reaches 93.2% with minimal NOx−.
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