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Influence of synthesis routes on oxygen content, crystallography, and thermal stability of Ti3AlC2 MAX phases and resulting MXenes

delete2025-09-11
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OA
AI
C
Chathushka D. Hettige Dharmasiri *
K
Konstantin L. Firestein *
J
Joseph F. S. Fernando
X
Xiaodong Wang
Z
Zhenhuan Chen
D
Dasun P. W. Guruge
C
Courtney‐Elyce M. Lewis
D
Dmitri Golberg *
DOI：10.1016/j.matdes.2025.114729delete
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Abstract

Abstract

En 中文
• Increased 1.8 Al molar ratio in planetary ball mill produces MAX phase with minimal impurities. • Transmission mode XRD allows to accurately calculate MXene lattice parameters and detects impurities. • Thermogravimetric studies show similar oxidation onsets around 460 °C for all MXenes. • In situ TEM heating reveals single MXene flake oxidation between 350 °C–420 °C.
Keywords:
Oxycarbide
MAX phase
MXenes
Thermal stability
Transmission XRD
In situ TEM heating
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M
Materials and Design
IF:
7.9
Papers:
1.9W
Citations:
9.8W

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