.png){kind=icon}
Return
Three-dimensional x-ray diffraction microscopy using high-energy x-rays
.png){kind=icon}
PRE
AI
DOI：10.1557/mrs2004.54.png)
.png){kind=icon}
Original request for help.png){kind=icon}
Share.png){kind=icon}
Save
Abstract
En 中文
Three-dimensional x-ray diffraction (3DXRD) microscopy is a tool for fast and nondestructive characterization of the individual grains, subgrains, and domains inside bulk materials. The method is based on diffraction with very penetrating hard x-rays (E greater than or equal to 50 keV), enabling 3D studies of millimeter-to-centimeter-thick specimens. The position, volume, orientation, and elastic and plastic strain can be derived for hundreds of grains simultaneously Furthermore, by applying novel reconstruction methods, 3D maps of the grain boundaries can be generated. The 3DXRD microscope in use at the European Synchrotron Radiation Facility in Grenoble, France, has a spatial resolution of similar to5 mum and can detect grains as small as 150 nm. The technique enables, for the first time, dynamic studies of the individual grains within polycrystalline materials. In this article, some fundamental materials science applications of 3DXRD are reviewed: studies of nucleation and growth kinetics during recrystallization, recovery, and phase transformations, as well as studies of polycrystal deformation.
Keywords:
high-energy x-rays
grain mapping
grain dynamics
three-dimensional x-ray diffraction microscopy
AI Summary
Key information extracted from the uploaded paper, including a brief overview, abstract, background, key highlights, visual analysis, and future outlook.
Journal
IF:
4.9
Papers:
5.3K
Citations:
9.5K
Organization
No organization information available
Cited Papers
Lattice rotations of individual bulk grains - Part I: 3D X-ray characterization.png)
ACTA MATERIALIA
ACTA MATERIALIAIF9.3
PREAI
ShareSave3D-characterisation of microstructure evolution during annealing of a deformed aluminum single crystalACTA MATERIALIA
ACTA MATERIALIAIF9.3
PREAI
ShareSave
Recrystallization kinetics of individual bulk grains in 90% cold-rolled aluminiumACTA MATERIALIA
ACTA MATERIALIAIF9.3
PREAI
ShareSaveShareSaveThe interaction of QDs with RAW264.7 cells: nanoparticle quantification, uptake kinetics and immune responses studyRSC Advances
RSC AdvancesIF0
PREAI
ShareSave
View more