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Solid-supported continuous flow synthesis in microreactors using electroosmotic flow
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DOI：10.1021/op049857x.png)
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This paper reports the fabrication of a microreactor suitable for use with supported reagents. We demonstrate that the electroosmotic flow can be used to move the reagents over a solid-supported catalyst bed. It is demonstrated that it is important that the support should not swell in organic solvents to obtain reproducible flow, and it is shown that silica supports fulfill this criteria. Silica-functionalised piperazine is used in a variety of Knoevenagel reactions to give the product in high conversion.
Keyword:
MICRO-REACTORS
REAGENTS
GLASS
期刊
O
IF:
3.5
论文数:
5.8K
被引数:
1.1W
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The use of a novel microreactor for high throughput continuous flow organic synthesis新型微反应器在高通量连续流有机合成中的应用
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