A Flow Reactor with Inline Analytics: Design and Implementation

Kristina Rita Somerville

doi:10.1021/op5002512

2014-10-24

PRE

Kristina Rita Somerville

DOI：10.1021/op5002512

原文链接

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摘要

En 中文

A continuous flow system complete with inline analytics is described. Sampling from a high pressure reactor and automated delivery mechanisms are detailed. The ability of the system to maintain critical process parameters (CPP) throughout a reaction process is demonstrated. Setup performance was evaluated using the Claisen rearrangement of allyl phenyl ether (1).

Keyword:

TRICYCLIC SULTAM LIBRARY

ORGANIC-SYNTHESIS MACOS

THIN-FILMS

TECHNOLOGY

GENERATION

GOLD

CYCLOADDITIONS

MICROREACTOR

CAPILLARIES

CHEMISTRY

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期刊

Organic Process Research and Development

IF:

3.5

论文数:

5.8K

被引数:

1.1W

机构

york university - canada

学者数:

8.3K

论文数: 9.0K

被引数: 10

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